MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\BIZ\\BIZ2017-106-WJ11.D Tgt Mass (EZX): 285.00 Injection Date : 6 Jan 17 3:08 pm +0800 Seq. Line : 0 Sample Name : BIZ2017-106-WJ11 Location : P2-C-05 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-13599 Batch#23178 Easy-Access Method: '1-POS-3MIN' 285.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off mAU20001500100050000.5*DAD1 C, Sig=254,4 Ref=off mAU40020000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.511.1981.1981.5271.7041.522.5min*1.65922.5min*2000001.14910000000.51 Ion 286, MSD1 286,Target Mass 285 +H Positive, EIC=285.7:286.7 1000075005000250000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.1781.522.5min1.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.20 0.02 965.98 1024.12 99.76 157 1.53 0.03 1.08 0.71 0.11 157 1.70 0.02 1.22 1.23 0.13 233 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.20 0.02 497.81 530.40 99.79 157 1.66 0.02 1.06 0.75 0.21 233HY-LCMS-02 1/6/2017 3:29:51 PM KFF(LCMS-02)Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.15 <<<< POSITIVE SPECTRA >>>> ES-API Positive2500020000150001000050000200300400500600700800900m/z 157.2HY-LCMS-02 1/6/2017 3:29:51 PM KFF(LCMS-02)
158.1 288.1 310.1Page 2 of 2
