MS Report from Instrument: LCMS-03 File ..3\\Data\\20171019\\20171019\\BIZ2017-O19-WYQ4.D Tgt Mass (CHM): Injection Date : 19 Oct 17 12:19 pm +0800 Seq. Line : 43 Sample Name : BIZ2017-O19-WYQ4 Location : P1-D-03 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20171019\\20171019\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20171019\\20171019\\1-POS-3MIN.M Catalog No : HY-13441 Batch#26749 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off1.3001.1411.180mAU200000.5 DAD1 B, Sig=254,4 Ref=offmAU500250000.5 ELS1 A, ELSD SignalmV0.306502511.3671..11531911.20211.3001.522.5min1.3601.4631.4902.0311.522.5min00.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7020000001000000000.51 Ion 292.1, MSD1 292.1,Target Mass 292.1 Positive, EIC=291.8:292.81.2481.3261.522.5min1.522.5min500000.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.14 0.02 0.93 1.00 0.24 311 1.18 0.01 1.29 0.01 0.34 311 1.30 0.02 377.29 412.68 99.42 293 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.14 0.02 0.61 0.54 0.07 311 1.15 0.02 0.35 0.32 0.04 311 1.20 0.02 1.48 1.47 0.17 311 1.30 0.02 856.36 887.30 99.55 293 1.36 0.01 0.48 0.79 0.06 293 1.46 0.02 0.12 0.14 0.01 293 1.49 0.02 0.37 0.22 0.04 293 2.03 0.01 0.51 0.56 0.06 105 Integration Results for MSD1 TIC, MS FileLCMS-03 10/19/2017 13:29:55 SYSTEMPage1 of4MS Report from Instrument: LCMS-03|-------|--------|--------------|--------------|--------|------| 1.25 0.10 1745710.50 287052.41 11.72 311 1.33 0.07 13148313.00 2932406.75 88.28 293 RetTim Width Area Height Area% MS(+)LCMS-03 10/19/2017 13:29:55 SYSTEMPage2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.25 <<<< POSITIVE SPECTRA >>>> ES-API Positive311.08000060000293.0225.1130.1294.0312.040000200000100200300400500600700800900m/zRet. Time: 1.33 ES-API Positive500000293.0311.04000003000002000001000000100200300400500600700800900m/zLCMS-03 10/19/2017 13:29:55 SYSTEMPage3 of4MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 10/19/2017 13:29:55 SYSTEMPage4 of4
